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Does microstructure matter for statistical nanoindentation techniques?

  • Franz Josef Ulm
  • , Matthieu Vandamme
  • , Hamlin M. Jennings
  • , James Vanzo
  • , Michelle Bentivegna
  • , Konrad J. Krakowiak
  • , Georgios Constantinides
  • , Christopher P. Bobko
  • , Krystyn J. Van Vliet
  • Massachusetts Institute of Technology
  • Université Paris-Est
  • Northwestern University
  • Universidade de Minho
  • Cyprus University of Technology
  • North Carolina State University

Research output: Contribution to journalComment/debate

166 Citations (Scopus)

Abstract

In their paper, Trtik et al. (2009) identify spurious peaks in the application of statistical nanoindentation technique as a critical obstacle for mechanical phase identification. In this discussion, we show that Trtik et al.'s finding is a consequence of an unrealistic virtual 3-D checkerboard microstructure considered by the authors. These peaks are not a general feature of indentation on multiphase materials, nor can the presence of such peaks be attributed to an intrinsic shortcoming of the grid-indentation technique. We also show that the authors' assertion of the absence of homogeneous material regions extending beyond 3 μm in cementitious materials is groundless.

Original languageEnglish
Pages (from-to)92-99
Number of pages8
JournalCement and Concrete Composites
Volume32
Issue number1
DOIs
Publication statusPublished - 1 Jan 2010
Externally publishedYes

Keywords

  • Microstructure
  • Nanoindentation
  • Statistical analysis

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