Effect of silane coupling agent on thermal stability and adhesion properties of DGEBF epoxy resin

Dong Su Lee; Seul Yi Lee; Byung Gak Min; Young Soo Seo; Bong Han Lee; Soo Jin Park

doi:10.7317/pk.2014.38.6.787

Effect of silane coupling agent on thermal stability and adhesion properties of DGEBF epoxy resin

Dong Su Lee
, Seul Yi Lee
, Byung Gak Min
, Young Soo Seo
, Bong Han Lee
, Soo Jin Park

Research output: Contribution to journal › Article › peer-review

Abstract

In this work, the epoxy specimens were prepared from diglycidyl ether of bisphenol F (DGEBF) with silane coupling agents (3-glycidoxypropyl trimethoxysilane (GPTMS)) in different ratios. Thermal stability was studied in terms of polymer decomposition temperature (PDT), temperature of maximum rate of weight loss (T_max), integral procedural decomposition temperature (IPDT), and decomposition activation energy (E_a) using TGA analysis. Adhesion properties of epoxy composite specimens were measured by UTM (universal testing machine) at atmosphere temperature. In this result, the adhesion properties of DGEBF were improved by addition of silane coupling agents compared to non-treated epoxy resin. However, when the content of GPTMS agent is more than 10 phr, adhesion properties decreased with increasing GPTMS agent.

Original language	English
Pages (from-to)	787-790
Number of pages	4
Journal	Polymer (Korea)
Volume	38
Issue number	6
DOIs	https://doi.org/10.7317/pk.2014.38.6.787
Publication status	Published - 1 Nov 2014
Externally published	Yes

Keywords

Adhesion properties
Epoxy resin
Silane coupling agent

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10.7317/pk.2014.38.6.787

Cite this

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title = "Effect of silane coupling agent on thermal stability and adhesion properties of DGEBF epoxy resin",

abstract = "In this work, the epoxy specimens were prepared from diglycidyl ether of bisphenol F (DGEBF) with silane coupling agents (3-glycidoxypropyl trimethoxysilane (GPTMS)) in different ratios. Thermal stability was studied in terms of polymer decomposition temperature (PDT), temperature of maximum rate of weight loss (Tmax), integral procedural decomposition temperature (IPDT), and decomposition activation energy (Ea) using TGA analysis. Adhesion properties of epoxy composite specimens were measured by UTM (universal testing machine) at atmosphere temperature. In this result, the adhesion properties of DGEBF were improved by addition of silane coupling agents compared to non-treated epoxy resin. However, when the content of GPTMS agent is more than 10 phr, adhesion properties decreased with increasing GPTMS agent.",

keywords = "Adhesion properties, Epoxy resin, Silane coupling agent",

author = "Lee, \{Dong Su\} and Lee, \{Seul Yi\} and Min, \{Byung Gak\} and Seo, \{Young Soo\} and Lee, \{Bong Han\} and Park, \{Soo Jin\}",

year = "2014",

month = nov,

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doi = "10.7317/pk.2014.38.6.787",

language = "English",

volume = "38",

pages = "787--790",

journal = "Polymer (Korea)",

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TY - JOUR

T1 - Effect of silane coupling agent on thermal stability and adhesion properties of DGEBF epoxy resin

AU - Lee, Dong Su

AU - Lee, Seul Yi

AU - Min, Byung Gak

AU - Seo, Young Soo

AU - Lee, Bong Han

AU - Park, Soo Jin

PY - 2014/11/1

Y1 - 2014/11/1

N2 - In this work, the epoxy specimens were prepared from diglycidyl ether of bisphenol F (DGEBF) with silane coupling agents (3-glycidoxypropyl trimethoxysilane (GPTMS)) in different ratios. Thermal stability was studied in terms of polymer decomposition temperature (PDT), temperature of maximum rate of weight loss (Tmax), integral procedural decomposition temperature (IPDT), and decomposition activation energy (Ea) using TGA analysis. Adhesion properties of epoxy composite specimens were measured by UTM (universal testing machine) at atmosphere temperature. In this result, the adhesion properties of DGEBF were improved by addition of silane coupling agents compared to non-treated epoxy resin. However, when the content of GPTMS agent is more than 10 phr, adhesion properties decreased with increasing GPTMS agent.

AB - In this work, the epoxy specimens were prepared from diglycidyl ether of bisphenol F (DGEBF) with silane coupling agents (3-glycidoxypropyl trimethoxysilane (GPTMS)) in different ratios. Thermal stability was studied in terms of polymer decomposition temperature (PDT), temperature of maximum rate of weight loss (Tmax), integral procedural decomposition temperature (IPDT), and decomposition activation energy (Ea) using TGA analysis. Adhesion properties of epoxy composite specimens were measured by UTM (universal testing machine) at atmosphere temperature. In this result, the adhesion properties of DGEBF were improved by addition of silane coupling agents compared to non-treated epoxy resin. However, when the content of GPTMS agent is more than 10 phr, adhesion properties decreased with increasing GPTMS agent.

KW - Adhesion properties

KW - Epoxy resin

KW - Silane coupling agent

UR - https://www.scopus.com/pages/publications/84919644849

U2 - 10.7317/pk.2014.38.6.787

DO - 10.7317/pk.2014.38.6.787

M3 - Article

AN - SCOPUS:84919644849

SN - 0379-153X

VL - 38

SP - 787

EP - 790

JO - Polymer (Korea)

JF - Polymer (Korea)

IS - 6

ER -

Effect of silane coupling agent on thermal stability and adhesion properties of DGEBF epoxy resin

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