Effects of injection conditions on dispersibility of TiO2 in polymerization of poly(ethylene terephthalate)

Seong Yoon Park; Hak Yong Kim; Fan Long Jin; Soo Jin Park

doi:10.5012/bkcs.2010.31.10.2893

Effects of injection conditions on dispersibility of TiO₂ in polymerization of poly(ethylene terephthalate)

Seong Yoon Park
, Hak Yong Kim
, Fan Long Jin
, Soo Jin Park

Chonbuk National University
Jilin Institute of Chemical Technology
Inha University

Research output: Contribution to journal › Article › peer-review

Abstract

In this study, the optimal preparation conditions in the polymerization process of poly(ethylene terephthalate) (PET) were studied in detail. As a result, the dispersibility of TiO₂ was significantly improved by the addition of dispersant and steric hinderance additives into TiO ₂/ethylene glycol (EG) slurry during the esterification step. The addition sequence of TiO₂/EG slurry and stirring also affected the dispersibility of TiO₂. The SEM results showed that some TiO ₂ particles were agglomerated in the PET matrix. The full dull (FD) PET chip and fiber were prepared according to the optimal preparation conditions. The FD PET fiber exhibited a better dispersibility than that of the FD PET chip.

Original language	English
Pages (from-to)	2893-2896
Number of pages	4
Journal	Bulletin of the Korean Chemical Society
Volume	31
Issue number	10
DOIs	https://doi.org/10.5012/bkcs.2010.31.10.2893
Publication status	Published - 20 Oct 2010
Externally published	Yes

Keywords

Chip
Dispersibility
Fiber
Poly(ethylene terephthalate)
TiO

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10.5012/bkcs.2010.31.10.2893

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title = "Effects of injection conditions on dispersibility of TiO2 in polymerization of poly(ethylene terephthalate)",

abstract = "In this study, the optimal preparation conditions in the polymerization process of poly(ethylene terephthalate) (PET) were studied in detail. As a result, the dispersibility of TiO2 was significantly improved by the addition of dispersant and steric hinderance additives into TiO 2/ethylene glycol (EG) slurry during the esterification step. The addition sequence of TiO2/EG slurry and stirring also affected the dispersibility of TiO2. The SEM results showed that some TiO 2 particles were agglomerated in the PET matrix. The full dull (FD) PET chip and fiber were prepared according to the optimal preparation conditions. The FD PET fiber exhibited a better dispersibility than that of the FD PET chip.",

keywords = "Chip, Dispersibility, Fiber, Poly(ethylene terephthalate), TiO",

author = "Park, \{Seong Yoon\} and Kim, \{Hak Yong\} and Jin, \{Fan Long\} and Park, \{Soo Jin\}",

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AU - Park, Seong Yoon

AU - Kim, Hak Yong

AU - Jin, Fan Long

AU - Park, Soo Jin

PY - 2010/10/20

Y1 - 2010/10/20

N2 - In this study, the optimal preparation conditions in the polymerization process of poly(ethylene terephthalate) (PET) were studied in detail. As a result, the dispersibility of TiO2 was significantly improved by the addition of dispersant and steric hinderance additives into TiO 2/ethylene glycol (EG) slurry during the esterification step. The addition sequence of TiO2/EG slurry and stirring also affected the dispersibility of TiO2. The SEM results showed that some TiO 2 particles were agglomerated in the PET matrix. The full dull (FD) PET chip and fiber were prepared according to the optimal preparation conditions. The FD PET fiber exhibited a better dispersibility than that of the FD PET chip.

AB - In this study, the optimal preparation conditions in the polymerization process of poly(ethylene terephthalate) (PET) were studied in detail. As a result, the dispersibility of TiO2 was significantly improved by the addition of dispersant and steric hinderance additives into TiO 2/ethylene glycol (EG) slurry during the esterification step. The addition sequence of TiO2/EG slurry and stirring also affected the dispersibility of TiO2. The SEM results showed that some TiO 2 particles were agglomerated in the PET matrix. The full dull (FD) PET chip and fiber were prepared according to the optimal preparation conditions. The FD PET fiber exhibited a better dispersibility than that of the FD PET chip.

KW - Chip

KW - Dispersibility

KW - Fiber

KW - Poly(ethylene terephthalate)

KW - TiO

UR - https://www.scopus.com/pages/publications/78049397738

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DO - 10.5012/bkcs.2010.31.10.2893

M3 - Article

AN - SCOPUS:78049397738

SN - 0253-2964

VL - 31

SP - 2893

EP - 2896

JO - Bulletin of the Korean Chemical Society

JF - Bulletin of the Korean Chemical Society

IS - 10

ER -

Effects of injection conditions on dispersibility of TiO₂ in polymerization of poly(ethylene terephthalate)

Abstract

Keywords

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