Further observations on the thermal stability of N-hydroxy-2-thiopyridone esters: improved decarboxylative radical additions to olefins

Jean Boivin; Elisabeth Crépon (née da Silva); Samir Z. Zard

doi:10.1016/0040-4039(91)80854-Y

Further observations on the thermal stability of N-hydroxy-2-thiopyridone esters: improved decarboxylative radical additions to olefins

Jean Boivin
, Elisabeth Crépon (née da Silva)
, Samir Z. Zard

Laboratoire de Synthèse Organique

Research output: Contribution to journal › Article › peer-review

Abstract

Decarboxylative radical addition onto olefins via thiohydroxamate esters can be considerably improved by heating and irradiating the reaction mixture; compound 10 can thus be obtained in 64% yield in one operation from acid chloride 6.

Original language	English
Pages (from-to)	199-202
Number of pages	4
Journal	Tetrahedron Letters
Volume	32
Issue number	2
DOIs	https://doi.org/10.1016/0040-4039(91)80854-Y
Publication status	Published - 7 Jan 1991
Externally published	Yes

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@article{bc80d9ea7c1d480d8e63218ae02673d4,

title = "Further observations on the thermal stability of N-hydroxy-2-thiopyridone esters: improved decarboxylative radical additions to olefins",

abstract = "Decarboxylative radical addition onto olefins via thiohydroxamate esters can be considerably improved by heating and irradiating the reaction mixture; compound 10 can thus be obtained in 64\% yield in one operation from acid chloride 6.",

author = "Jean Boivin and \{Cr{\'e}pon (n{\'e}e da Silva)\}, Elisabeth and Zard, \{Samir Z.\}",

year = "1991",

month = jan,

day = "7",

doi = "10.1016/0040-4039(91)80854-Y",

language = "English",

volume = "32",

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journal = "Tetrahedron Letters",

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T1 - Further observations on the thermal stability of N-hydroxy-2-thiopyridone esters

T2 - improved decarboxylative radical additions to olefins

AU - Boivin, Jean

AU - Crépon (née da Silva), Elisabeth

AU - Zard, Samir Z.

PY - 1991/1/7

Y1 - 1991/1/7

N2 - Decarboxylative radical addition onto olefins via thiohydroxamate esters can be considerably improved by heating and irradiating the reaction mixture; compound 10 can thus be obtained in 64% yield in one operation from acid chloride 6.

AB - Decarboxylative radical addition onto olefins via thiohydroxamate esters can be considerably improved by heating and irradiating the reaction mixture; compound 10 can thus be obtained in 64% yield in one operation from acid chloride 6.

UR - https://www.scopus.com/pages/publications/0026011069

U2 - 10.1016/0040-4039(91)80854-Y

DO - 10.1016/0040-4039(91)80854-Y

M3 - Article

AN - SCOPUS:0026011069

SN - 0040-4039

VL - 32

SP - 199

EP - 202

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 2

ER -

Further observations on the thermal stability of N-hydroxy-2-thiopyridone esters: improved decarboxylative radical additions to olefins

Abstract

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