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Toward a new lower limit for the minimum scattering vector on the very small angle neutron scattering spectrometer at Laboratoire Léon Brillouin

  • Annie Brûlet
  • , Vincent Thévenot
  • , Didier Lairez
  • , Sébastien Lecommandoux
  • , Willy Agut
  • , Steven P. Armes
  • , Jianzong Du
  • , Sylvain Désert
  • Institut Pierre Simon Laplace, CNRS and CEA
  • Ecole Nationale Supérieure de Chimie et de Physique de Bordeaux
  • Department of Chemistry
  • The University of Sheffield

Résultats de recherche: Contribution à un journalArticleRevue par des pairs

24 Citations (Scopus)

Résumé

The main characteristics of the very small angle neutron scattering spectrometer (VSANS) under construction at the Laboratoire Léon Brillouin are a multibeam pinhole collimator converging onto an image plate detector. By combining tiny collimation (diaphragms of around 1 or 2 mm in diameter) with the small pixel size of the detector (0.15 × 0.15 mm), very high resolution measurements can be achieved. The resolution function of the instrument contains a contribution from gravity, which is reduced by the intermediate masks of the collimator. Owing to the relatively short length of the VSANS instrument (around 14 m), this effect remains weak, in good agreement with the predictions. With a prototype multibeam collimator, an incident wavelength of 0.9 nm and the detector located at 6 m from the sample, it is possible to access q values as low as 4 × 10-3 nm-1 with very high q resolution. Promising preliminary experiments with high q resolution are reported, which open up new fields to the SANS technique.

langue originaleAnglais
Pages (de - à)161-166
Nombre de pages6
journalJournal of Applied Crystallography
Volume41
Numéro de publication1
Les DOIs
étatPublié - 16 janv. 2008
Modification externeOui

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